Formation of N-nitrosodimethylamine during the Storage of ranitidine reagent powder

oegterm

Temperature-dependent formation of N-nitrosodimethylamine in the course of the storage of ranitidine reagent powders and tablets

The aim of this research was to elucidate the impact of high-temperature storage on the steadiness of ranitidine, particularly with respect to the potential formation of N-nitrosodimethylamine (NDMA), which is classed as a possible human carcinogen.
Commercially obtainable ranitidine reagent powders and formulations have been saved beneath numerous situations, and subjected to LC-MS/MS evaluation. When ranitidine tablets from two completely different manufacturers (designated as pill A and pill B) have been saved beneath accelerated situation (40°C with 75% relative humidity), following the drug stability pointers issued by the Worldwide Convention on Harmonisation (ICH-Q1A), for as much as eight weeks, the quantity of NDMA in them considerably elevated from 0.19 to 116 ppm and from 2.89 to 18 ppm, respectively.
The formation of NDMA that exceeded the appropriate each day consumption restrict (0.32 ppm) on the temperature used beneath accelerated storage situations clearly highlights the danger of NDMA formation in ranitidine formulations when extrapolated to storage beneath ambient situations.
A forced-degradation research beneath the stress situation (60°C for 1 week) strongly instructed that environmental elements comparable to moisture and oxygen are concerned within the formation of NDMA in ranitidine formulations. Storage of ranitidine tablets and reagent powders on the excessive temperatures additionally elevated the quantity of nitrite, which is taken into account one of many elements influencing NDMA formation.
These information point out the need of controlling/monitoring stability-related elements, along with controlling impurities in the course of the manufacturing course of, with a view to mitigate nitrosamine-related well being dangers of sure prescribed drugs.

Human Free PSA (f-PSA) ELISA Kit

PRB-5049-FREE-5 5 x 96 assays
EUR 2739.6

Human Serum (Troponin I Free)

90R-106 100 ml
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Serum Albumin, Lipid Free Protein

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Bovine Serum Albumin, protease free

GK4012-1KG 1 kg
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Bovine Serum Albumin, protease free

GK4012-500G 500 g
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PK15 Cell Serum-Free Medium

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500mL Insectagro DS2 Serum-Free

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500mL INSECTAGRO SF9 serum free

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B-27 Serum-Free Supplement (50x)

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This non-canonical electrophilic amino acid can subsequently be addressed selectively by way of bioorthogonal Hydrazino- iso -Pictet-Spengler (HIPS) or Knoevenagel ligation to connect payloads like fluorophores or medicine to proteins, whereas acquiring an outlined payload-to-protein ratio.
Nonetheless, disadvantages of those conjugation strategies embrace the necessity of a big extra of conjugation constructing block, comparably low response charges and restricted stability of FGly-containing proteins.
Due to this fact, functionalized clickable HIPS and tandem Knoevenagel constructing blocks have been synthesized, conjugated to small proteins (DARPins) and subsequently linked to strained alkyne-containing payloads for protein labeling. This process allowed the selective bioconjugation of 1 or two DBCO-carrying payloads with almost stoichiometric quantities at low concentrations.
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EUR 169.2

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E04S0014-48 1 plate of 48 wells
EUR 624
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E04S0228-192T 192 tests
EUR 1524
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E04S0228-48 1 plate of 48 wells
EUR 624
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E04S0228-96 1 plate of 96 wells
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E04S0273-192T 192 tests
EUR 1524
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EUR 358.8

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Rabbit Serum Albumin Polyclonal Antibody

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EUR 117.7

Rabbit Serum Albumin Polyclonal Antibody

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Rabbit Serum Albumin Polyclonal Antibody

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EUR 423.5

Rabbit Serum Albumin Polyclonal Antibody

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  • EUR 684.66
  • EUR 117.70
  • EUR 302.50
  • EUR 423.50
  • 100 µg
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VACUETTE Bleeding with Gel Activator Serum 8ml Greiner VACUETTE Bleeding with Gel Activator Serum 8ml Greiner

455071A PK50
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Cow Serum

abx098251-100ml 100 ml
EUR 410.4

Fish Serum

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EUR 526.8

Goat Serum

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EUR 444

Goat Serum

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Horse Serum

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EUR 410.4

Mouse Serum

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EUR 155407.2

Mouse Serum

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  • EUR 326.40
  • 100 ml
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Mouse Serum

abx098261-5L 5 L
EUR 10599.6

Mouse Serum

abx098262-1ml 1 ml
EUR 2064

Porcine Serum

abx098264-1L 1 L
EUR 710.4

Rat Serum

abx098267-10ml 10 ml
EUR 326.4

Sheep Serum

abx098268-100ml 100 ml
EUR 410.4

Canine Serum

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EUR 184.8
Description: Non Sterile Canine Serum

Equine Serum

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EUR 240

Chicken Serum

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EUR 318

Glycated Bovine Serum Albumin (BSA) with ?-Galactose

SPR-203A 0.05 mg
EUR 372
Description: Untagged synthetic panspecies Galactose BSA Glycoconjugate for WB, ELISA. The biological activity of this protein has not yet been tested.

Glycated Bovine Serum Albumin (BSA) with ?-Galactose

SPR-203B 2x0.05 mg
EUR 548.4
Description: Untagged synthetic panspecies Galactose BSA Glycoconjugate for WB, ELISA. The biological activity of this protein has not yet been tested.

Glycated Bovine Serum Albumin (BSA) with ?-Galactose

SPR-203C 4x0.05 mg
EUR 783.6
Description: Untagged synthetic panspecies Galactose BSA Glycoconjugate for WB, ELISA. The biological activity of this protein has not yet been tested.

Glycated Bovine Serum Albumin (BSA) with ?-Glucose

SPR-204A 0.05 mg
EUR 372
Description: Untagged synthetic panspecies Glucose BSA Glycoconjugate for WB, ELISA. The biological activity of this protein has not yet been tested.

Glycated Bovine Serum Albumin (BSA) with ?-Glucose

SPR-204B 2x0.05 mg
EUR 548.4
Description: Untagged synthetic panspecies Glucose BSA Glycoconjugate for WB, ELISA. The biological activity of this protein has not yet been tested.

Glycated Bovine Serum Albumin (BSA) with ?-Glucose

SPR-204C 4x0.05 mg
EUR 783.6
Description: Untagged synthetic panspecies Glucose BSA Glycoconjugate for WB, ELISA. The biological activity of this protein has not yet been tested.

Bovine Serum Albumin (BSA) modified with Acrolein

SPR-206A 0.05 mg
EUR 307.2
Description: Untagged synthetic panspecies Acrolein BSA Conjugate for WB, ELISA. The biological activity of this protein has not yet been tested.

Bovine Serum Albumin (BSA) modified with Acrolein

SPR-206B 2x0.05 mg
EUR 444
Description: Untagged synthetic panspecies Acrolein BSA Conjugate for WB, ELISA. The biological activity of this protein has not yet been tested.

Bovine Serum Albumin (BSA) modified with Acrolein

SPR-206C 4x0.05 mg
EUR 627.6
Description: Untagged synthetic panspecies Acrolein BSA Conjugate for WB, ELISA. The biological activity of this protein has not yet been tested.

Bovine Serum Albumin (BSA) modified with Crotonaldehyde

SPR-207A 0.05 mg
EUR 372
Description: Untagged synthetic panspecies Crotonaldehyde BSA Conjugate for WB, ELISA. The biological activity of this protein has not yet been tested.

Bovine Serum Albumin (BSA) modified with Crotonaldehyde

SPR-207B 2x0.05 mg
EUR 548.4
Description: Untagged synthetic panspecies Crotonaldehyde BSA Conjugate for WB, ELISA. The biological activity of this protein has not yet been tested.

Bovine Serum Albumin (BSA) modified with Crotonaldehyde

SPR-207C 4x0.05 mg
EUR 783.6
Description: Untagged synthetic panspecies Crotonaldehyde BSA Conjugate for WB, ELISA. The biological activity of this protein has not yet been tested.

Bovine Serum Albumin (BSA) modified with Methylglyoxal

SPR-208A 0.05 mg
EUR 307.2
Description: Untagged synthetic panspecies Methylglyoxal BSA Conjugate for WB, ELISA. The biological activity of this protein has not yet been tested.

Bovine Serum Albumin (BSA) modified with Methylglyoxal

SPR-208B 2x0.05 mg
EUR 444
Description: Untagged synthetic panspecies Methylglyoxal BSA Conjugate for WB, ELISA. The biological activity of this protein has not yet been tested.

Bovine Serum Albumin (BSA) modified with Methylglyoxal

SPR-208C 4x0.05 mg
EUR 627.6
Description: Untagged synthetic panspecies Methylglyoxal BSA Conjugate for WB, ELISA. The biological activity of this protein has not yet been tested.

Bovine Serum Albumin (BSA) modified with Malondialdehyde

SPR-209A 0.05 mg
EUR 307.2
Description: Untagged synthetic panspecies Malondialdehyde BSA Conjugate for WB, ELISA. The biological activity of this protein has not yet been tested.

Bovine Serum Albumin (BSA) modified with Malondialdehyde

SPR-209B 2x0.05 mg
EUR 444
Description: Untagged synthetic panspecies Malondialdehyde BSA Conjugate for WB, ELISA. The biological activity of this protein has not yet been tested.

Bovine Serum Albumin (BSA) modified with Malondialdehyde

SPR-209C 4x0.05 mg
EUR 627.6
Description: Untagged synthetic panspecies Malondialdehyde BSA Conjugate for WB, ELISA. The biological activity of this protein has not yet been tested.

Human Serum thiol(Serum thiol) ELISA Kit

YLA3776HU-48T 48T
EUR 435

Human Serum thiol(Serum thiol) ELISA Kit

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EUR 562.5

anti-Rpn3 (yeast) antibody, rabbit serum

62-201 100uL
EUR 543.6
Description: The anti-Rpn3 (yeast) antibody, rabbit serum is available in Europe and for worldwide shipping via Gentaur.

Anti-Streptolysin O antibody rabbit serum

64-001 50uL
EUR 496.8
Description: The Anti-Streptolysin O antibody rabbit serum is available in Europe and for worldwide shipping via Gentaur.

anti-Rad18 (human) antibody, rabbit serum

70-023 50uL
EUR 496.8
Description: The anti-Rad18 (human) antibody, rabbit serum is available in Europe and for worldwide shipping via Gentaur.

Bovine Serum Albumin / BSA Rabbit mAb

A11625-100ul 100 ul
EUR 492

Bovine Serum Albumin / BSA Rabbit mAb

A11625-200ul 200 ul
EUR 685.2

Bovine Serum Albumin / BSA Rabbit mAb

A11625-20ul 20 ul
EUR 265.2

Bovine Serum Albumin / BSA Rabbit mAb

A11625-50ul 50 ul
EUR 344.4

Rabbit Serum NS TH MT 500mL

31116-5 500mL
EUR 235.91

Rabbit Serum NH S DELIPID. 500mL

31117-5 500mL
EUR 358.57

Rabbit Serum NS NH YG 100mL

31118-1 100mL
EUR 211.12

Rabbit Serum NS NH YG 3L

31118-3 3L
EUR 1148.1

Rabbit Serum NS NH YG 500mL

31118-5 500mL
EUR 306.37

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