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Configuration of Cyclic Amines with Bode’s Acylation Reagents
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A bis(silylene)-stabilized diphosphorus compound and its reactivity as a monophosphorus anion switch reagent
In distinction to the well-established transition-metal-mediated activation of white phosphorus (P4), the metal-free direct functionalization of P4 has remained uncommon. The conversion of P4 right into a reactive zero-valent diphosphorus compound (P2) has confirmed difficult to hold out with out counting on steel reactivity.
Herein, we describe the facile degradation of P4 mediated by two divalent silicon atoms in a bis(silylene) scaffold, leading to a silylene-stabilized zero-valent P2 advanced.
The presence of two lone pairs of electrons on every P atom within the silylene-stabilized P2 advanced allows a wealthy reactivity in direction of small molecules; response of the P2 species with CO2, water or a borane results in the formation of P-C, P-H or P-B bonds, respectively. Notably, the P2 advanced additionally serves as a single phosphorus anion (P–) switch reagent in direction of steel carbonyls and a chlorogermylene compound, resulting in the synthetically helpful phosphaketenide (PCO–) ligand and a phosphinidene germylene advanced, respectively.
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OPEF01351-100G - Human Serum Albumin Antigen Reagent Grade |
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Albumin Bovine (pH 7) fraction V Reagent Grade (Bovine Serum Albumin, BSA), 99% |
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Description: Part B |
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Description: CryoProtX Mix Reagents 1.5 mL |
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Set of 10 Biolipidure Reagents |
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| Biolipidure-set | AS ONE International | 10mLx10 | EUR 1820.4 |
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Description: Set of 10 Biolipidure Reagents, whose applications include Immunoassays, Western blots, Immunohistochemistry, Turbidimetric assays, Immunochromatography, and Bead based assays. Benefits include: No lot to lot variation, No animal derived materials, Non-specific adsorption suppression, Stabilization of immobilized antibody, Stabilization of enzyme-antibody conjugate, Enzyme-substrate reaction enhancement and aggregation reaction enhancement |
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Mouse Serum Proteins goat polyclonal antibody, Serum |
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| AP31483SU-N | Origene Technologies GmbH | 1 ml | Ask for price |
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High Range Ammonia Reagents - EACH |
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Mouse Serum Proteins rabbit polyclonal antibody, Serum |
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Mouse Serum - 100 ml |
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CryoProtX Mix Eco Reagents 1.5 mL |
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| M-MDSR-61-ECO | MiTeGen | 1.5 ml ml | EUR 37 |
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Description: CryoProtX Mix Eco Reagents 1.5 mL |
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PeliKine tool set, additional reagents |
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| M1980 | Tecan Benelux | 1 unit | EUR 169.8 |
Mouse Serum Amyloid P Component (SAP) Reference serum |
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Normal Mouse Serum |
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| 88-NM35 | Fitzgerald | 50 ml | EUR 459 |
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Description: Normal Mouse Serum |
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Normal Mouse Serum |
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| 88R-1002 | Fitzgerald | 5 ml | EUR 118 |
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Description: Normal Mouse Serum which has been lipid extracted and dialyzed against 10 mM Sodium Phosphate, 0.15 M Sodium Chloride, pH 7.2 |
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Normal Mouse Serum |
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| BMS0070-10mL | Abbkine | 10 mL | EUR 89 |
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Description: High quality Normal mouse serum processed from non-immunized normal adult mouses is used as a blocking agent or as a negative control for immunoassays. |
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Normal Mouse Serum |
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| BMS0070-10mL10 | Abbkine | 10 mL×10 | EUR 529 |
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Description: High quality Normal mouse serum processed from non-immunized normal adult mouses is used as a blocking agent or as a negative control for immunoassays. |
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| BMS0070-each | Abbkine | each | Ask for price |
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| MBS539323-50mL | MyBiosource | 50mL | EUR 710 |
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Mouse Serum Albumin |
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| 30R-3304 | Fitzgerald | 10 mg | EUR 153 |
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Description: Purified native Mouse Serum Albumin |
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Haptoglobin, Mouse Serum |
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Utilizing the Competing Enantioselective Conversion Methodology to Assign the Absolute Configuration of Cyclic Amines with Bode’s Acylation Reagents
The competing enantioselective conversion (CEC) methodology is a fast and dependable means to find out absolute configuration. Beforehand, Bode’s chiral acylated hydroxamic acids had been used to find out the stereochemistry of main amines, in addition to cyclic and acyclic secondary amines. The enantioselective acylation has been evaluated for 4-, 5-, and six-membered cyclic secondary amines, together with medicinally related compounds.
The constraints of the strategy had been studied by way of computational evaluation and experimental outcomes. Piperidines with substituents on the 2-position didn’t behave nicely except the axial conformer was energetically accessible, which is per the transition state geometries proposed by Bode and Kozlowski.
Management experiments had been carried out to analyze the reason for degrading selectivity below the CEC response circumstances. The current examine expands the scope of the CEC methodology for secondary amines and offers a greater understanding of the response profile.
Synthesis of Alkyl Silanes through Response of Unactivated Alkyl Chlorides and Triflates with Silyl Lithium Reagents
The response of unactivated secondary and first alkyl chlorides in addition to main alkyl triflates with silyl lithium reagents to entry tetraorganosilanes is reported. These nucleophilic substitutions proceed within the absence of any transition steel catalyst below delicate circumstances in average to excellent yields. The silyl lithium reagents are readily generated from the corresponding commercially obtainable chlorosilanes. Enantioenriched secondary alkyl chlorides react with excessive stereospecificity below inversion of configuration.
Floor-enhanced Raman Scattering Detection of Nucleic Acids exhibiting Sterically Accessible Guanines utilizing Ruthenium-polypyridyl Reagents
Right here, we report the applying of surface-enhanced Raman scattering (SERS) spectroscopy as a speedy and sensible device for assessing the formation of coordinative adducts between nucleic acid guanines and ruthenium polypyridyl reagents. The know-how offers a sensible method for the wash-free and fast identification of nucleic acid buildings exhibiting sterically accessible guanines.
That is demonstrated for the detection of a quadruplex-forming sequence current within the promoter area of the c-myc oncogene, which reveals a non-paired, reactive guanine at a flanking place of the G-quartets.
A DFT Examine on Fe I/Fe II/Fe III Mechanism of the Cross-Coupling between Haloalkane and Aryl Grignard Reagent Catalyzed by Iron-SciOPP Complexes
To discover believable response pathways of the cross-coupling response between a haloalkane and an aryl steel reagent catalyzed by an iron-phosphine advanced, we look at the response of FeBrPh(SciOPP) <b>1</b> and bromocycloheptane using density purposeful concept (DFT) calculations.
Moreover the cross-coupling, we additionally examined the aggressive pathways of β-hydrogen elimination to provide the corresponding alkene byproduct. The DFT examine on the response pathways explains the cross-coupling selectivity over the elimination by way of Fe<sup>I</sup>/Fe<sup>II/</sup>Fe<sup>III</sup> mechanism which includes the era of alkyl radical intermediates and their propagation in a series response method.
The current examine offers perception into the detailed molecular mechanic of the cross-coupling response and revises the Fe<sup>II</sup>/Fe<sup>II</sup> mechanisms beforehand proposed by us and others
ExoQualiTM Overall Exosome Isolation Reagent (from serum) |
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| CEIK-044L-30T | Creative Bioarray | 30 T | Ask for price |
ExoQualiTM Overall Exosome Isolation Reagent (from serum) |
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| CEIK-044L-50T | Creative Bioarray | 50 T | Ask for price |
Albumin Depletion Reagent for Plasma and Serum (10 ml) NEW! |
|||
| P5W13 | 101Bio | 10 rxn | EUR 99 |
OPEF01351-100G - Human Serum Albumin Antigen Reagent Grade |
|||
| OPEF01351-100G | Aviva Systems Biology | 100g | EUR 1302 |
Bovine Serum Albumin Fatty Acid Protease Free Reagent Grade |
|||
| GWB-DCC190 | GenWay Biotech | 1 kg | Ask for price |
MinuteTM Albumin Depletion Reagent for Plasma and Serum (20 ml) |
|||
| WA-013 | Inventbiotech | each | EUR 135 |
Albumin Bovine (pH 7) fraction V Reagent Grade (Bovine Serum Albumin, BSA), 99% |
|||
| 65186 | Sisco Laboratories | 10 Gms | EUR 38.4 |
|
Description: Part B |
|||
MOUSE SERUM Serum Products |
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| GWB-Q00006 | GenWay Biotech | 100 ml | Ask for price |
EZ-DNA Reagents |
|||
| SK8201 | Bio Basic | 100preps | EUR 112.2 |
Ecl Detection Reagents |
|||
| RPN3004 | Scientific Laboratory Supplies | EACH | EUR 552.9 |
Ecl Detection Reagents - EACH |
|||
| RPN2105 | Scientific Laboratory Supplies | EACH | EUR 815.4 |
Mouse Serum |
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| abx098261-100L | Abbexa | 100 L | EUR 600 |
Mouse Serum |
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| 20-abx098261 | Abbexa |
|
|
Mouse Serum |
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| abx098261-1ml | Abbexa | 1 ml | Ask for price |
Mouse Serum |
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| abx098261-200l | Abbexa | 200 µl | Ask for price |
Mouse Serum |
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| abx098261-5L | Abbexa | 5 L | EUR 10599.6 |
Mouse Serum |
|||
| abx098262-1ml | Abbexa | 1 ml | EUR 2064 |
Mouse serum |
|||
| IHR-8141 | ImmunoBioscience | 10 ml | EUR 47.75 |
Mouse Serum |
|||
| M2021-050 | GenDepot | 500ml | EUR 970 |
MOUSE SERUM |
|||
| MBS238224-100mL | MyBiosource | 100mL | EUR 845 |
MOUSE SERUM |
|||
| MBS238224-5x100mL | MyBiosource | 5x100mL | EUR 3620 |
Mouse Serum - 100ml |
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| MO-340/100 | Biosera France - Medical Scientific Equipment | 100ml | EUR 183.32 |
Mouse Serum - 500ml |
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| MO-340/500 | Biosera France - Medical Scientific Equipment | 500ml | EUR 733.32 |
MOUSE SERUM WITH 0.09% AZIDE Serum Products |
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| GWB-Q00007 | GenWay Biotech | 5 ml | Ask for price |
MOUSE SERUM WITH 0.09% AZIDE Serum Products |
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| GWB-Q00008 | GenWay Biotech | 10 ml | Ask for price |
MOUSE SERUM WITH 0.09% AZIDE Serum Products |
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| GWB-Q00009 | GenWay Biotech | 50 ml | Ask for price |
Serum, Mouse |
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| MBS638822-100mL | MyBiosource | 100mL | EUR 815 |
Serum, Mouse |
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| MBS638822-5x100mL | MyBiosource | 5x100mL | EUR 3435 |
CryoProtX Mix Reagents 1.5 mL |
|||
| M-MDSR-61 | MiTeGen | 1.5 ml ml | EUR 37 |
|
Description: CryoProtX Mix Reagents 1.5 mL |
|||
Set of 10 Biolipidure Reagents |
|||
| Biolipidure-set | AS ONE International | 10mLx10 | EUR 1820.4 |
|
Description: Set of 10 Biolipidure Reagents, whose applications include Immunoassays, Western blots, Immunohistochemistry, Turbidimetric assays, Immunochromatography, and Bead based assays. Benefits include: No lot to lot variation, No animal derived materials, Non-specific adsorption suppression, Stabilization of immobilized antibody, Stabilization of enzyme-antibody conjugate, Enzyme-substrate reaction enhancement and aggregation reaction enhancement |
|||
Mouse Serum Proteins goat polyclonal antibody, Serum |
|||
| AP31483SU-N | Origene Technologies GmbH | 1 ml | Ask for price |
REAGENTS HIGH RANGE AMMONIA - PK25 |
|||
| HI73325 | Scientific Laboratory Supplies | PK25 | EUR 55.35 |
High Range Ammonia Reagents - EACH |
|||
| HI9373301 | Scientific Laboratory Supplies | EACH | EUR 130.95 |
Mouse Serum Proteins rabbit polyclonal antibody, Serum |
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| AP31472SU-N | Origene Technologies GmbH | 1 ml | Ask for price |
Mouse Serum - 100 ml |
|||
| CAMOU-1B | Westburg | each | EUR 554.28 |
CryoProtX Mix Eco Reagents 1.5 mL |
|||
| M-MDSR-61-ECO | MiTeGen | 1.5 ml ml | EUR 37 |
|
Description: CryoProtX Mix Eco Reagents 1.5 mL |
|||
PeliKine tool set, additional reagents |
|||
| M1980 | Tecan Benelux | 1 unit | EUR 169.8 |
Mouse Serum Amyloid P Component (SAP) Reference serum |
|||
| SAP12-RS | Alpha Diagnostics | 100 ul | EUR 388.8 |
Mouse Serum pool |
|||
| MBS571968-1mL | MyBiosource | 1mL | EUR 160 |
Mouse Serum pool |
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| MBS571968-5x1mL | MyBiosource | 5x1mL | EUR 575 |
Mouse Serum - 10ml |
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| MO-340/10 | Biosera France - Medical Scientific Equipment | 10ml | EUR 28.11 |
Mouse Serum - 20ml |
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| MO-340/20 | Biosera France - Medical Scientific Equipment | 20ml | EUR 55 |
Mouse Serum - 50ml |
|||
| MO-340/50 | Biosera France - Medical Scientific Equipment | 50ml | EUR 97.79 |
Alkphos Direct Labelling Reagents - EACH |
|||
| RPN3680 | Scientific Laboratory Supplies | EACH | EUR 915.3 |
Normal Mouse Serum |
|||
| 88-NM35 | Fitzgerald | 50 ml | EUR 459 |
|
Description: Normal Mouse Serum |
|||
Normal Mouse Serum |
|||
| 88R-1002 | Fitzgerald | 5 ml | EUR 118 |
|
Description: Normal Mouse Serum which has been lipid extracted and dialyzed against 10 mM Sodium Phosphate, 0.15 M Sodium Chloride, pH 7.2 |
|||
Normal Mouse Serum |
|||
| BMS0070-10mL | Abbkine | 10 mL | EUR 89 |
|
Description: High quality Normal mouse serum processed from non-immunized normal adult mouses is used as a blocking agent or as a negative control for immunoassays. |
|||
Normal Mouse Serum |
|||
| BMS0070-10mL10 | Abbkine | 10 mL×10 | EUR 529 |
|
Description: High quality Normal mouse serum processed from non-immunized normal adult mouses is used as a blocking agent or as a negative control for immunoassays. |
|||
Normal Mouse Serum |
|||
| BMS0070-each | Abbkine | each | Ask for price |
Normal Mouse Serum |
|||
| MBS539323-50mL | MyBiosource | 50mL | EUR 710 |
Normal Mouse Serum |
|||
| MBS539323-5x50mL | MyBiosource | 5x50mL | EUR 2975 |
Normal Mouse Serum |
|||
| MBS686158-5mL | MyBiosource | 5mL | EUR 180 |
Normal Mouse Serum |
|||
| MBS686158-5x5mL | MyBiosource | 5x5mL | EUR 655 |
Normal Mouse Serum |
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| MBS686304-2mL | MyBiosource | 2mL | EUR 150 |
Normal Mouse Serum |
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| MBS686304-5x2mL | MyBiosource | 5x2mL | EUR 535 |
Normal Mouse Serum |
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| MBS9718943-10mL | MyBiosource | 10mL | EUR 135 |
Normal Mouse Serum |
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| MBS9718943-10x10mL | MyBiosource | 10x10mL | EUR 395 |
Normal Mouse Serum |
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| NMS | Complement Technology | 1 ml/vial | EUR 91 |
Normal Mouse Serum |
|||
| MBS837810-5mL | MyBiosource | 5mL | EUR 300 |
Normal Mouse Serum |
|||
| MBS837810-5x5mL | MyBiosource | 5x5mL | EUR 1210 |
Mouse Serum Albumin |
|||
| 30R-3304 | Fitzgerald | 10 mg | EUR 153 |
|
Description: Purified native Mouse Serum Albumin |
|||
Mouse Serum Albumin |
|||
| CSB-NP000801m | Cusabio | 10mg | Ask for price |
Mouse Serum albumin |
|||
| MBS571996-10mg | MyBiosource | 10mg | EUR 395 |
Mouse Serum albumin |
|||
| MBS571996-5x10mg | MyBiosource | 5x10mg | EUR 1625 |
Mouse Serum Albumin |
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| MBS7615609-INQUIRE | MyBiosource | INQUIRE | Ask for price |
Mouse Serum Albumin |
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| MBS717450-100mg | MyBiosource | 100mg | EUR 635 |
Mouse Serum Albumin |
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| MBS717450-10mg | MyBiosource | 10mg | EUR 180 |
Mouse Serum Albumin |
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| MBS717450-1g | MyBiosource | 1g | EUR 2930 |
Mouse Serum Albumin |
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| MBS717450-1mg | MyBiosource | 1mg | EUR 135 |
Mouse Serum Albumin |
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Serum, Mouse, Normal |
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Serum, Mouse, Normal |
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| MBS638791-5mL | MyBiosource | 5mL | EUR 475 |
Serum, Mouse, Normal |
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| MBS638791-5x5mL | MyBiosource | 5x5mL | EUR 1990 |
Serum, Mouse, Normal |
|||
| MBS638800-05mL | MyBiosource | 0.5mL | EUR 465 |
Serum, Mouse, Normal |
|||
| MBS638800-5x05mL | MyBiosource | 5x0.5mL | EUR 1950 |
Serum, Mouse, Normal |
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Serum, Mouse, Normal |
|||
| MBS638811-5x5mL | MyBiosource | 5x5mL | EUR 2125 |
Haptoglobin, Mouse Serum |
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| MBS173102-01mg | MyBiosource | 0.1mg | EUR 865 |
Haptoglobin, Mouse Serum |
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| MBS173102-1mg | MyBiosource | 1mg | EUR 2650 |
Haptoglobin, Mouse Serum |
|||
| MBS173102-5x1mg | MyBiosource | 5x1mg | EUR 11715 |
Free Chlorine Reagents 0-5mg/L - EACH |
|||
| WAT1028 | Scientific Laboratory Supplies | EACH | EUR 49.95 |
Mouse Complement Serum |
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| 32R-CM001 | Fitzgerald | 5 ml | EUR 526 |
|
Description: Frozen high activity mouse complement serum |
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